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EPMA

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Chemical composition of the pristine clay and the clay-based catalysts was determined using an electron probe micro-analyzer (EPMA) JXA-8800R (JEOL) Before EPMA measurements, all the samples were dried at 80[degrees]C under vacuum to remove absorbed water, and then the clays were molded into a shape of disk.
ACKNOWLEDGEMENTS We are thankful to Teemu Ohman at Oulu University for his help with SEM and EPMA studies and to Matti Leino and Satu Vuoriainen of the Laboratory of Geophysics, Geological Survey of Finland, for their help with using the equipment.
Subsequently, XRD and EPMA techniques were used to determine the corrosion products and elemental distribution for optimized MCrAlY and 300 [micro]m thick TBC after hot corrosion studies.
 
 
 
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