Different materials like dichloromethane, n- hexane, charcoal, column silica gel, TLC cards, ethyl acetate, Na metal, NaOH, methanol, ethanol, 1- propanol, 2-propanol, 1-butanol, 1-pentanol, 1- hexanol, benzyl alcohol, chloroform and toluene were used for the experimental purpose.
The reactivity order of alcohols was observed to be methanol greater than ethanol greater than benzyl alcohol greater than 1-propanolgreater than 1-butanol greater than 1-pentanol greater than 1-hexanol greater than 2- propanol.
The reagents used to prepare the micellar mobile phases were SDS (99% purity), 1-propanol, 1-butanol, 1-pentanol
, disodium hydrogen phosphate, and HCl (Merck).
2002), de los coeficientes de actividad del 1-pentanol
con los de los pentanodioles son muy altas.
Henry's law constants and infinite dilution activity coefficients of propane, propene, butane, isobutane, 1-butene, isobutene, trans-2-butene, and 1,3-butadiene in 1-pentanol, 2-pentanol, and 3-pentanol.
Henry's law constants and infintite dilution activity coefficients of cis-2-butene, dimethylether, chloroethane, and 1,1-difluoroethane in methanol, 1-propanol, 2-propanol, 1-butanol, 2-butanol, isobutanol, tert-butanol, 1-pentanol, 2-pentanol, 3-pentanol, 2-methyl-l-butanol, 3-methyl-l-butanol, and 2-methyl-2-butanol.
33 3-Methyl-2-butanone, 1-pentanol
, 2,3-dichloro-l-propene, >30 1,2,4-tifluorobenzene, 1-butanol, 2-pentanol, 1,3-dichlorotetrafluoro-2-propanone, 1,4-dioxane, n-propyl acetate, methoxyflurane (pentrane), 4-methyl-2-pentanone, 2-chloroethyl-ethyl ether, dibromomethane, cyclopropyl methyl ketone, tetrachloroethylene, 2-Chloro-2-methyl-2-propanol Table 3.
Styrene, divinyl benzene (DVB), sodium dodecyl sulfate (SDS), azobisisobutyronitrile (AIBN), and 1-pentanol were purchased from Sigma Aldrich and used without further purification.
476 g of SDS and 2 ml of 1-pentanol in 200 ml of deionized water and sonicated for 4 h.
Commercial TTIP, 1-pentanol, and DEOA were purchased from Wako Pure Chemical Industries, Ltd.
Deionized water, 1-pentanol, and DEOA were mixed in a separable flask with a condenser connected to a trap.