(5) 2,2,6,6-Tetramethylpiperidinyloxy benzoic acid (3.4 g, 9.4 mmol) was coupled with [beta]-CD ([beta]-cyclodextrin 8.6 g, 7.0 mmol) using dicyclohexylcarbodiimide
(DCC 2.1 g, 9.5mmol) in DMF (dimethylformamide 100 mL).
(25) Modification of Glu190 of the [beta] subunit of T[F.sub.1] (from thermophilic Bacillus PS3) with dicyclohexylcarbodiimide
(DCCD) (26) and substitution of this residue by glutamine (27) resulted in complete loss of the activity.
N, N'- dicyclohexylcarbodiimide
(DCC) (34.05 g, 0.165 mol) dissolved in ethyl acetate (60 mL) was added to the cooled ethyl acetate solution at 0[degrees]C.
Folate (FA), dicyclohexylcarbodiimide
(DCC), N-hydroxysuccinimide (NHS), dioxotetrahydrofuran, and 4-dimethylaminopyridine (DMAP) were purchased from Aladdin Industrial Co.
Various methods have already been reported for the synthesis of indole-3-acetamides including the usage of various coupling reagents like DCC (N,N- dicyclohexylcarbodiimide
). However, the use of DCC results in the production of o-acylurea which may undergo rearrangement leading to the formation of un-reactive intermediate N-acylurea consequently yield is reduced.
Stannous octoate (Sn-oct, Sigma), Dicyclohexylcarbodiimide
(DCC, FLUCA), 4-(dimethyl amino) pyridine (DMAP, FALUCA), dichloromethane (DCM), Dimethyl Sulphoxide (DMSO) and other chemicals used in the current investigation were of HPLC grade procured from Ranbaxy Fine Chemicals Ltd, India.
, an inhibitor of proton translocators, inhibited the NADPH '!
Mechanism of inhibition of mitochondrial adenosine triphosphatase by dicyclohexylcarbodiimide
and oligomycin: relationship to ATP synthesis.
Compound 5a (9.8 mg; 1.9 [micro]mol) and N-hydroxysuccinimide (2.2 mg; 1.9 [micro]mol) were dissolved in 100 [micro]L of anhydrous DMF, and dicyclohexylcarbodiimide
(3.9 mg; 1.9 [micro]mol) was added last.
was purchased from J&K Scientific.
Briefly, to a 0.2mL solution of PMLA (25mg, 0.22 mmol equivalent of malic acid) in acetone was added a mixture of N-hydroxysuccinimide (NHS, 25 mg, 0.22 mmol) and dicyclohexylcarbodiimide
(DCC, 47 mg, 0.22 mmol) in 0.2 mL DMF.
Synthesis of fatty acid anhydrides by reaction with dicyclohexylcarbodiimide
. J Lipid Res 1966;7:174-95.