Platinum and a saturated calomel electrode
(SCE) were used as counter and reference electorde, respectively.
The electrochemical cell assembly used in the present investigation is of 500ml capacity equipped with a saturated calomel electrode
and platinum electrode which served as reference electrode and auxiliary electrode respectively.
Ltd); magnetic stirring apparatus (model: RCT basic; IKA); electronic contact temperature control meter (model: ETS-D5; IKA); saturated calomel electrode
(model: 217; Shanghai precision scientific instrument Co.
The electrobath used in the electrolysis test consisted of a conductive, coated electrode (the working electrode), a platinum electrode (the counter electrode), and a saturated calomel electrode
(the reference electrode), and is depicted in Fig.
A saturated calomel electrode
(SCE) was used as reference and a Pt foil served as the auxiliary electrode.
The Waveform Generator PP RI, HITEK instruments England, UK with potentiostat, X-Y recorder and cell assembly possessing GCBE/GCME as working electrode, Pt as an auxiliary electrode and saturated calomel electrode
(SCE) as a reference electrode were used for voltammetric determination of silver.
2] immerging in 3% NaCl solution, and a saturated calomel electrode
was used as reference, and a platinum as counter electrode.